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Simplify elemental analysis with rapid microwave acid digestion. The most advanced microwave systems and vessels available for acid digestion.

Jan 07, 1986· Briefly, an apparatus for continuously concentrating and denitrating a nitrate solution by using microwave according to the present invention has a basic construction in which a concentrating and denitrating vessel rotatably supported is disposed within an oven into which microwave is applied through waveguide means.

Demonstration of pyropartitioning technology by denitration and chlorination experiment using real highlevel liquid waste Central Research Institute of Electric Power Industry (Japan) Koichi UOZUMI, Masatoshi IIZUKA, Masaki KURATA, Tadashi INOUE Institute for Transuranium Elements (ECJRC) Michel OUGIER, Rikard MALMBECK, and JeanPaul GLATZ

1. Denitration Reaction It is widely recognized that dielectrics are internally heated up in a microwave electrical field. The MH method is such a process that PuU nitrate solution is heated up, concentrated and then denitrated to MOX powder by 1000 microwave energy. Process steps on the de

Nov 14, 2011· CEM Microwave Digestion System Model Star System 6, Process up to 6 samples independently using different methods at simultaneous or sequential start .

fluorocarbon polymer (PFA or TFM) or quartz microwave vessel or vessel liner. The vessel is sealed and heated in the microwave unit for a specified period of time. After cooling, the vessel contents are filtered, centrifuged, or allowed to settle and then diluted to volume and analyzed by the appropriate determinative method. DEFINITIONS ...

The ETHOS UP fully embodies Milestone''s philosophy in microwave sample preparation. Specifically designed for closed vessel microwave acid digestion, it offers productivity, safety, ease of use, connectivity, expertise and application flexibility.

Microwave Chemistry in Organic Synthesis (By A. Bacher, UCLA, ) Introduction The serendipitous discovery that microwave technology can be used for cooking is based on a melted candy bar in the discoverer''s pocket, Percy Spencer, a Raytheon engineer. In .

The Synergy™ software and onboard controls of the Discover make it the easiesttouse microwave system, even for those who have little or no experience with microwave technology in the laboratory, while still maintaining all of the advanced programming options requested by skilled microwave users.

and slags in minutes! Available liners: Teflon, Pyrex®, or quartz. HP500 Plus HP500 Plus vessels are ideal for routine digestion applications. Process up to 14 highpressure vessels per run with temperatures up to 260 °C or pressures up to 500 psi. Available liners: Teflon, Pyrex®, or quartz. Omni One vessel does it all!

Vessels The most advanced vessels ever made. CEM manufactures a wide variety of vessels to meet the temperature and pressure conditions required to completely digest your samples. All CEM vessels are manufactured from materials that are microwave transparent and focus all .

However, such researches have not been reported. Microwave energy has not been used to these fields despite so many applications of microwaves in nuclear chemistry and engineering. This may be because of the research of metals leaching is still on the age of laboratory scale and has not been applied to the industry widely.

fluorocarbon polymer (PFA or TFM) or quartz microwave vessel or vessel liner. The vessel is sealed and heated in the microwave unit for a specified period of time. After cooling, the vessel contents are filtered, centrifuged, or allowed to settle and then diluted to volume and analyzed by the appropriate determinative method. DEFINITIONS

The efficient microwave energy transfer to the feedstock in the bed is another important issue related to the microwave reactor. The reactor vessel, made of materials transparent to microwaves ( quartz), must be carefully and appropriately cleaned, especially at continuous operation mode.

Advanced Microwave Muffle Furnace. The new Milestone PYRO is an advanced microwave muffle furnace ashing system of new generation. PYRO perfectly suits several applications including ashing, sulfated ashing, loss on ignition (LOI), residue on ignition (ROI), fusion and generally all hightemperature reactions under controlled conditions.

Before subjecting vessels to microwave energy the vessels should be free of particulate matter or drops of liquid such as high salt solutions that can absorb microwaves, which in turn can cause localized heating and damage to the vessel. Pressure relief devices should always be .

Process samples completely unattended. The Discover SPD is more than the latest technology for microwave digestion: it is a new concept in sample preparation. Discover SPD is a sequential, pressurized microwave digestion system that processes samples completely unattended, allowing laboratory staff to tend to other tasks.

A microwave oven (Multiwave 3000 microwave sample preparation system, Anton Paar, Graz, Austria) equipped with eight highpressure quartz vessels was used in the experiments. The internal volume of vessels was 80 mL and the maximum operational temperature and pressure were set at 280 °C and 80 bar, respectively.

The ultraWAVE operates up to 199 bar pressure and 300°C. Unlike traditional microwave digestion systems, every sample is under direct temperature and pressure control. This eliminates the reliance on a reference vessel or indirect control such as infrared temperature sensors, assuring complete control of the digestion process in every sample.

Sineo has incorporated the latest technology of material design while engineering a very safe, durable and easy to use microwave. The quartz digestion vessel enables the digestion process to be visible; Initiative wireless remote video monitoring system, together with quartz vessels, makes the reaction be seen clearly at a glance.

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A number of accessories are available to help the analyst get the most out of the ETHOS UP. Milestone offers a variety of inserts in different materials (Quartz or TFM) and with various sizes and shapes, accommodating a vast array of applications. Both quartz vessels and insert options are available for the SK15 and MAXI44 rotors.

The conversion of solid samples into representative solutions is the first step for the analytical procedure. By using microwave technology it is possible to heat up the sample solution extremely fast and perform digestions at high pressures and temperatures, due to the applied pressure vessels even far above the boiling point of the used acids.

ATMOSPHERIC PRESSURE PLASMA MICROWAVE PROCESSING ... Figure 2 below shows plasma that is contained within a quartz vessel. Note in particular the ... which enables good observation of the process ...
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